Forensic Engineers and Consultants

Archive: Boilers and Pressure Vessels

Interpreting Industrial Incident Data – Lesson Learned

This is a case study about an incident I investigated involving a major upset in a distillation column.  This blog builds on the previous blogs about the Distributed Control System, DCS – Data is the Key.

Distillation is a method of separating mixtures of compounds with differing boiling points.  Uncle Bill with his still on the hill separates ethanol, that boils at 173°F, from water that boils at 212°F.  If the mixture is heated to above 173°F, but below 212°F, the ethanol will boil, the vapor will travel up out of the unit and then can be condensed and served over ice with an olive…   Any mixture of two or more chemicals with different boiling points can be separated in this way.  The distillation Read More

What Does a Recovery Boiler Recover? – Quite a bit, actually!

The Kraft paper process was invented in 1879 and produces a stronger finished product that other paper manufacturing methods. One of the waste streams is known as black liquor and is a mixture of solids and water.  It contains lignin, hemicelluloses and chemicals used in the pulping process. The original process had no use for this harmful waste stream and it was dumped into nearby waterways, to their detriment!!!  Mr. G.H. Tomlinson invented the recovery boiler in the early 1930’s.  This development made the Kraft process the manufacturing method of choice, as explained below. Read More

Heat Exchanger Failures Will Shut Your Process Down

Heat exchangers, as the name implies, are used to bring a process stream to a desired temperature.  They can heat or cool either gases or liquids. They are fairly intricate in their construction, therefore not the cheapest piece of equipment to purchase.  For that reason, facilities don’t keep “spare” exchangers lying around, so when they fail catastrophically, the entire manufacturing process goes down with them… and stays down until they are fixed or replaced. Ow!

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Ammonia – The Good, The Bad, The Smelly… Part Two

Now that you know what ammonia is (see Part One here), how it behaves, and how to safely store it and work with it, let’s look at some areas in industry where it is used.

Anhydrous ammonia has a use in pollution control.  Industrial boilers and power plants burn coal or natural gas to make steam and/or electricity. When the fuel is burned using air as the oxygen source nitrogen gets exposed to the heat as well because air is 79% nitrogen.  The nitrogen gets oxidized and forms several compounds referred to as NOx (NO, NO2, NO3).  NOx compounds are harmful to Read More

Ammonia

Ammonia – The Good, The Bad, The Smelly… Part One

Ammonia is a compound consisting of one nitrogen atom and three hydrogen atoms and is denoted by the formula NH3. Its boiling point is -28°F at atmospheric pressure, so unless it is under pressure, it is gaseous at room temperatures. Therefore, pure ammonia is typically stored under pressure in a liquid form. Household ammonia is only 5-10% NH3, the remaining 90-95% is water. Ammonia is extremely soluble in water. It is often depicted  like this: Read More

Testing As Part of Gas Appliance Incident Investigation

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Equipment and appliances supplied with fuel gases like natural gas, propane and butane are a common and convenient part of most of our lives.  Such devices as gas grills and ranges, ovens, furnaces, space heaters and water heaters usually perform without incident.  However, when they malfunction the potential for incidents such as fires and explosions, carbon monoxide (CO) poisoning and burn injuries may occur. These incidents may be due to design and manufacturing defects in the product, or improper installation or operation of the device.

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Chemical Engineers: More than Glorified Plumbers – Really!

As a senior at Virginia Tech, I was told that ChemE’s were little more than glorified plumbers.  Looking back, I’m pretty sure it was to keep our geek-egos in check. It was an effective tool! However, as I grew and traveled as a professional, it became an effective descriptor; applying to a larger scale and using a modifier or two for specific applications.  So, if you have a loss that falls into one of the categories below, a ChemE could be the expert you need. Read More

Graphitic Corrosion – Difficult to determine before a failure!

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Graphitic corrosion is a process that may happen in equipment made of iron, particularly grey cast iron, but also ductile cast iron. Graphitic corrosion can lead to unexpected catastrophic failure of the affected part because the cast iron can lose its strength without a visible warning such as a change in size, shape, or appearance. Read More

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